1, 2, 4-Triazines. III the methylation of 5, 6-dimethyl-l, 2, 4-triazin- 3-amine and related compounds and the identification of the products by carbon-13 nuclear magnetic resonance spectroscopy

Jacobsen N.W. and de Jonge I. (1987) 1, 2, 4-Triazines. III the methylation of 5, 6-dimethyl-l, 2, 4-triazin- 3-amine and related compounds and the identification of the products by carbon-13 nuclear magnetic resonance spectroscopy. Australian Journal of Chemistry, 40 12: 1979-1988. doi:10.1071/CH9871979


Author Jacobsen N.W.
de Jonge I.
Title 1, 2, 4-Triazines. III the methylation of 5, 6-dimethyl-l, 2, 4-triazin- 3-amine and related compounds and the identification of the products by carbon-13 nuclear magnetic resonance spectroscopy
Journal name Australian Journal of Chemistry   Check publisher's open access policy
ISSN 1445-0038
Publication date 1987-01-01
Sub-type Article (original research)
DOI 10.1071/CH9871979
Open Access Status Not yet assessed
Volume 40
Issue 12
Start page 1979
End page 1988
Total pages 10
Language eng
Subject 1600 Chemistry
Abstract 5, 6-Dimethyl-l, 2, 4-triazin-3-amine reacts with methyl iodide to give 3-amino-1, 5, 6-trimethyl- 1, 2, 4-triazinium iodide and 2, 5, 6-trimethyl-1, 2, 4-triazin-3(2H)-imine hydriodide. The products were identified by classical methods and confirmed by C n.m.r. spectroscopy to establish this as a reliable technique for determining the sites of methylation in such systems. The methylation products from other alkyl- and aryl-substituted l, 2, 4-triazin-3-amines are also reported.
Q-Index Code C1
Q-Index Status Provisional Code
Institutional Status Unknown

Document type: Journal Article
Sub-type: Article (original research)
Collection: Scopus Import - Archived
 
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Created: Tue, 25 Jul 2017, 00:03:52 EST by System User