A furnace for x-ray diffraction studies of single crystals

Lucas B.W. (1973) A furnace for x-ray diffraction studies of single crystals. Journal of Physics E: Scientific Instruments, 6 11: 1097-1099. doi:10.1088/0022-3735/6/11/025


Author Lucas B.W.
Title A furnace for x-ray diffraction studies of single crystals
Journal name Journal of Physics E: Scientific Instruments   Check publisher's open access policy
ISSN 0022-3735
Publication date 1973-01-01
Sub-type Article (original research)
DOI 10.1088/0022-3735/6/11/025
Volume 6
Issue 11
Start page 1097
End page 1099
Total pages 3
Subject 2200 Engineering
3100 Physics and Astronomy
3105 Instrumentation
Abstract A miniature furnace suitable for the collection of single crystal x-ray diffraction data at temperatures between room temperature and about 200°C is described. The device was primarily designed for solid-state phase transformation investigations, but may be used for general diffraction studies. Commercially available goniometer heads require only minor modification to allow attachment of the furnace. The sample can be maintained for periods of up to several weeks with a temperature constancy to within ± 1°C. The integral arrangement of the goniometer head and furnace allows transferability of the unit, whilst maintaining the sample temperature. The region of reciprocal space normally accessible for data collection is not significantly reduced by use of the furnace.
Q-Index Code C1
Q-Index Status Provisional Code
Institutional Status Unknown

Document type: Journal Article
Sub-type: Article (original research)
Collection: Scopus Import - Archived
 
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Created: Tue, 28 Jun 2016, 17:16:09 EST by System User