Gas-liquid chromatography of vitamin D as trimethylsilyl derivatives

Fisher A.L., Parfitt A.M. and Lloyd H.M. (1972) Gas-liquid chromatography of vitamin D as trimethylsilyl derivatives. Journal of Chromatography A, 65 3: 493-499. doi:10.1016/S0021-9673(00)84995-X


Author Fisher A.L.
Parfitt A.M.
Lloyd H.M.
Title Gas-liquid chromatography of vitamin D as trimethylsilyl derivatives
Journal name Journal of Chromatography A   Check publisher's open access policy
ISSN 0021-9673
Publication date 1972-03-01
Sub-type Article (original research)
DOI 10.1016/S0021-9673(00)84995-X
Volume 65
Issue 3
Start page 493
End page 499
Total pages 7
Subject 1602 Criminology
Abstract Investigation of several column packing materials for the gas-liquid chromatographic analysis of vitamin D as the trimethylsilyl (TMS) derivatives showed that 4% OV-225 on High Performance Chromosorb W, 100-120 mesh, was the most suitable. The TMS derivatives were found to be unstable, but adequate reproducibility was achieved, using cholestane as the internal standard, by standardizing the time between silylation and injection.
Q-Index Code C1
Q-Index Status Provisional Code
Institutional Status Unknown

Document type: Journal Article
Sub-type: Article (original research)
Collection: Scopus Import
 
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Created: Sat, 09 Jul 2016, 07:41:19 EST by System User